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B031957 - APPLIED ANALYTICAL CHEMISTRY WITH LABORATORY
Main information
Teaching Language
Learning Objectives
Course Content
Prerequisites
Teaching Methods
Type of Assessment
Course program
Suggested readings
Further information
Academic Year 2023-24
Coorte 2022 - 3-years First Cycle Degree (DM 270/04) in CHIMICA
Course year
Second year - First Semester
Belonging Department
Chemistry "Ugo Schiff"
Course Type
Single education field course
Scientific Area
CHIM/01 - ANALYTICAL CHEMISTRY
Credits
6
Teaching Hours
56
Teaching Term
11/09/2023 ⇒ 22/12/2023
Attendance required
No
Type of Evaluation
Final Grade
Course Content
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Course program
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Lectureship
Teaching Language
Italian
Learning Objectives
The course supplies to the student thorough knowledge of several instrumental analytical techniques.
Course Content (Search our library's catalogue)
Data analysis. Electrochemical techniques: potentiometry, voltammetry. Spectrophotometry in UV-vis. Atomic Absorbance: fundamentals and instrumentation.
Fundamentals of separation techniques.
Fundamentals of separation techniques.
Prerequisites
Analytical chemistry I, Laboratory of analytical Chemistry I.
Teaching Methods
Total number of hours for lectures: 32.
Total number of hours for Laboratory-field practice: 24.
Total number of hours for Laboratory-field practice: 24.
Type of Assessment
Laboratory reports of the exercises carried out.
Oral examination.
Oral examination.
Course program
Analytical quality criteria and performance tests. Calibration curve. Electrochemical techniques: potentiometry, voltammetry.
Spectrophotometry theory.
Instruments for optical spectroscopy. Molecular absorption spectroscopy. Atomic spectroscopy.
Introduction to analytical separations.
Theory and instrumentation of Gas-Chromatography. Columns and stationary phases. Liquid chromatography. HPLC: theory and instrumentation. Column and stationary phases, isocratic and gradient elution, detectors, applications. Ionic chromatography: principles and instrumentation. Exclusion dimensional chromatography: theory and applications.
Spectrophotometry theory.
Instruments for optical spectroscopy. Molecular absorption spectroscopy. Atomic spectroscopy.
Introduction to analytical separations.
Theory and instrumentation of Gas-Chromatography. Columns and stationary phases. Liquid chromatography. HPLC: theory and instrumentation. Column and stationary phases, isocratic and gradient elution, detectors, applications. Ionic chromatography: principles and instrumentation. Exclusion dimensional chromatography: theory and applications.
Suggested readings
Fundamentals of Analytical Chemistry; Skoog, West, Holler, Saunders Publishing. Quantitative Chemical Analysis 9th Edition Daniel C. Harris.
Further information
Slides of the topics covered in the course are available on Moodle.